产品介绍:
TSKgel HHR 色谱柱
主要特点:
TSKgel HHR 系列色谱柱的zui高使用温度是 140 ºC。
TSKgel HHR 系列色谱柱的溶剂范围较宽,所有色谱柱出货溶剂都为THF,也可置换成多种有机溶剂。可置换的溶剂种类在下表中列出。
TSKgel HHR 系列色谱柱是规格为7.8 mm ID x 30 cm 的常规GPC色谱柱。
TSKgel HHR 色谱柱的校准曲线
出货溶剂 | 置换溶剂 |
四氢呋喃 | 丙酮、乙醇、喹啉、苯、邻二氯苯、乙酸乙酯、十二烷、 FC-113、四氯化碳5、二氯甲烷、二氯乙烷、三氯乙烷、正己烷、环己烷、 二甲苯、四氢呋喃、氯仿、1,4-二噁烷、六氟异丙醇、甲苯、1-氯萘、N、 N-二甲基乙酰基乙酰胺、jia基乙基酮、三氯苯、间甲酚、二甲基甲酰胺、 甲基吡咯烷酮、邻氯苯酚/氯仿、二甲基亚砜、吡啶 |
注意事项:
TSKgel SuperH 和 HHR 色谱柱置换溶剂时,请参照下表中列出的建议流速。一旦置换成丙酮等强极性溶剂,不建议再置换回非极性溶剂。
TSKgel HXL、HHR、SuperHZ、SuperH 型色谱柱的出货溶剂都是四氢呋喃(THF)、高温色谱柱(HT)的出货溶剂是邻二氯苯(ODCB)。
长时间暴露在四氯化碳中,会腐蚀色谱柱和HPLC系统的不锈钢部件。
* TSKgel H 系列色谱柱不可用于100% 甲醇;若使用该溶剂,应选择TSKgel SW 系列或 Alpha 系列色谱柱。
** TSKgel H 系列色谱柱可在订购时指定出货溶剂。
线性校准型色谱柱
溶剂 | 建议流速 |
正己烷 | 0.9 |
jia基乙基酮 | 0.7 |
二氯甲烷、乙酸乙酯 | 0.6 |
甲苯、氯仿 | 0.5 |
二甲基甲酰胺 | 0.4 |
四氯化碳、吡啶 | 0.3 |
二甲基亚砜、二噁烷、乙醇 N-甲基吡咯烷酮、邻二氯苯 | 0.2 |
喹啉、六氟异丙醇、1-氯萘 | 0.1 |
推荐溶剂 |
应用范围 |
THF (四氢呋喃) | 聚苯乙烯、环氧树脂、苯氧基树脂、聚碳酸酯、 聚异戊二烯、聚乙酸乙烯酯、聚氯乙烯、 聚甘油单酯、脂肪酸、聚丁二烯、 聚(甲基丙烯酸酯)、聚(苯乙烯-丁二烯)、 聚(苯乙烯-丙烯腈) |
二甲基甲酰胺(DMF) +/- 5mM LiBr | 聚氯乙烯、聚氟乙烯、尿素树脂、 聚氨酯、聚苯乙烯、聚酯、 聚酰亚胺醚、聚酰亚胺酯、 多酚 (水溶液)、聚丙烯腈 |
邻二氯苯 (ODCB) | 聚乙烯、聚丙烯 |
氯仿 | 醚类聚羧酸、丙烯酸树脂、环氧树脂、 聚苯乙烯 |
间甲酚 / 氯仿 | 尼龙、聚酯、 聚酰胺、聚对苯二甲酸乙二酯 |
甲苯 | 聚丁二烯、聚硅氧烷 |
TSKgel G1000HHR
Matrix: | polystyrene-divinylbenzene |
Particle Size (mean): | 5 µm |
Pore size (mean): | 1.5 nm |
Exclusion Limit: | < 1,000 Da |
Max. Temp. (ºC): | 140 |
Shipping Solvent: | THF for 0017352 and 0017368 Chloroform for 0018270 and 0018271 |
P/N | Description | Particle size | Housing material | ID (mm) | Length (cm) |
0017352 | TSKgel G1000HHR | 5 µm | Stainless Steel | 7.8 | 30 |
0017368 | Guard Column for P/N 0017352 | 5 µm | Stainless Steel | 6 | 4 |
0018270 | TSKgel G1000HHR | 5 µm | Stainless Steel | 21.5 | 30 |
0018271 | Guard Column for P/N 0018270 | 5 µm | Stainless Steel | 7.5 | 7.5 |
TSKgel G2000HHR
Matrix: | polystyrene-divinylbenzene |
Particle Size (mean): | 5 µm |
Pore size (mean): | 2 nm |
Exclusion Limit: | < 10,000 Da |
Max. Temp. (ºC): | 140 |
Shipping Solvent: | THF for 0017353 and 0017368 Chloroform for 0018259 and 0018271 |
P/N | Description | Particle size | Housing material | ID (mm) | Length (cm) |
0017353 | TSKgel G2000HHR | 5 µm | Stainless Steel | 7.8 | 30 |
0017368 | Guard Column for P/N 0017353 | 5 µm | Stainless Steel | 6 | 4 |
0018259 | TSKgel G2000HHR | 5 µm | Stainless Steel | 21.5 | 30 |
0018271 | Guard Column for P/N 0018259 | 5 µm | Stainless Steel | 7.5 | 7.5 |
TSKgel G2500HHR
Matrix: | polystyrene-divinylbenzene |
Particle Size (mean): | 5 µm |
Pore size (mean): | 3 nm |
Exclusion Limit: | 20,000 Da |
Max. Temp. (ºC): | 140 |
Shipping Solvent: | THF for 0017354 and 0017368 Chloroform for 0018266 and 0018271 |
P/N | Description | Particle size | Housing material | ID (mm) | Length (cm) |
0017354 | TSKgel G2500HHR | 5 µm | Stainless Steel | 7.8 | 30 |
0017368 | Guard Column for P/N 0017354 | 5 µm | Stainless Steel | 6 | 4 |
0018266 | TSKgel G2500HHR | 5 µm | Stainless Steel | 21.5 | 30 |
0018271 | Guard Column for P/N 0018266 | 5 µm | Stainless Steel | 7.5 | 7.5 |
TSKgel G3000HHR
Matrix: | polystyrene-divinylbenzene |
Particle Size (mean): | 5 µm |
Pore size (mean): | 7.5 nm |
Exclusion Limit | 60,000 Da |
Max. Temp. (ºC): | 140 |
Shipping Solvent: | THF for 0017355 and 0017368 Chloroform for 0018267 and 0018271 |
P/N | Description | Particle size | Housing material | ID (mm) | Length (cm) |
0017355 | TSKgel G3000HHR | 5 µm | Stainless Steel | 7.8 | 30 |
0017368 | Guard Column for P/N 0017355 | 5 µm | Stainless Steel | 6 | 4 |
0018267 | TSKgel G3000HHR | 5 µm | Stainless Steel | 21.5 | 30 |
0018271 | Guard Column for P/N 0018267 | 5 µm | Stainless Steel | 7.5 | 7.5 |
TSKgel G4000HHR
Matrix: | polystyrene-divinylbenzene |
Particle Size (mean): | 5 µm |
Pore size (mean): | 20 nm |
Exclusion Limit: | < 400,000 Da |
Max. Temp. (ºC): | 140 |
Shipping Solvent: | THF for 0017356 and 0017368 Chloroform for 0018268 and 0018271 |
P/N | Description | Particle size | Housing material | ID (mm) | Length (cm) |
0017356 | TSKgel G4000HHR | 5 µm | Stainless Steel | 7.8 | 30 |
0017368 | Guard Column for P/N 0017356 | 5 µm | Stainless Steel | 6 | 4 |
0018268 | TSKgel G4000HHR | 5 µm | Stainless Steel | 21.5 | 30 |
0018271 | Guard Column for P/N 0018268 | 5 µm | Stainless Steel | 7.5 | 7.5 |
TSKgel G5000HHR
Matrix: | polystyrene-divinylbenzene |
Particle Size (mean): | 5 µm |
Pore size (mean): | 65 nm |
Exclusion Limit: | < 4 x 106 Da |
Max. Temp. (ºC): | 140 |
Shipping Solvent: | THF |
P/N | Description | Particle size | Housing material | ID (mm) | Length (cm) |
0017357 | TSKgel G5000HHR | 5 µm | Stainless Steel | 7.8 | 30 |
0017369 | Guard Column for P/N 0017357 | 5 µm | Stainless Steel | 6 | 4 |
TSKgel G6000HHR
Matrix: | polystyrene-divinylbenzene |
Particle Size (mean): | 5 µm |
Pore size (mean): | ND |
Exclusion Limit: | < 4 x 107 Da |
Max. Temp. (ºC): | 140 |
Shipping Solvent: | THF |
P/N | Description | Particle size | Housing material | ID (mm) | Length (cm) |
0017358 | TSKgel G6000HHR | 5 µm | Stainless Steel | 7.8 | 30 |
0017369 | Guard Column for P/N 0017358 | 5 µm | Stainless Steel | 6 | 4 |
TSKgel G7000HHR
Matrix: | polystyrene-divinylbenzene |
Particle Size (mean): | 5 µm |
Pore size (mean): | ND |
Exclusion Limit: | 4 x 108 Da |
Max. Temp. (ºC): | 140 |
Shipping Solvent: | THF |
P/N | Description | Particle size | Housing material | ID (mm) | Length (cm) |
0017359 | TSKgel G7000HHR | 5 µm | Stainless Steel | 7.8 | 30 |
0017369 | Guard Column for P/N 0017359 | 5 µm | Stainless Steel | 6 | 4 |
TSKgel GMHHR-H mixed-bed
Matrix: | polystyrene-divinylbenzene |
Particle Size (mean): | 5 µm |
Pore size (mean): | ND |
Exclusion Limit: | < 4 x 108 Da |
Max. Temp. (ºC): | 140 |
Shipping Solvent: | THF for 0017360 and 0017369 Chloroform for 0018269 and 0018272 |
P/N | Description | Particle size | Housing material | ID (mm) | Length (cm) |
0017360 | TSKgel GMHHR-H | 5 µm | Stainless Steel | 7.8 | 30 |
0017369 | Guard column for P/N 0017360 | 5 µm | Stainless Steel | 6 | 4 |
0018269 | TSKgel GMHHR-H | 5 µm | Stainless Steel | 21.5 | 30 |
0018272 | Guard column for P/N 0018269 | 5 µm | Stainless Steel | 7.5 | 7.5 |
TSKgel GMHHR-M mixed bed
Matrix: | polystyrene-divinylbenzene |
Particle Size (mean): | 5 µm |
Pore size (mean): | mixed |
Exclusion Limit: | < 4 x 106 Da |
Max. Temp. (ºC): | 140 |
Shipping Solvent: | THF |
P/N | Description | Particle size | Housing material | ID (mm) | Length (cm) |
0017392 | TSKgel GMHHR-M | 5 µm | Stainless Steel | 7.8 | 30 |
0017369 | Guard Column for P/N 0017392 | 5 µm | Stainless Steel | 6 | 4 |
TSKgel GMHHR-N
Matrix: | polystyrene-divinylbenzene |
Particle Size (mean): | 5 µm |
Pore size (mean): | mixed |
Exclusion Limit: | < 400,000 Da |
Max. Temp. (ºC): | 140 |
Shipping Solvent: | THF |
P/N | Description | Particle size | Housing material | ID (mm) | Length (cm) |
0018055 | TSKgel GMHHR-N | 5 µm | Stainless Steel | 7.8 | 30 |
0017369 | Guard Column for P/N 0018055 | 5 µm | Stainless Steel | 6 | 4 |
TSKgel GMHHR-L mixed bed
Matrix: | polystyrene-divinylbenzene |
Particle Size (mean): | 5 µm |
Pore size (mean): | mixed |
Exclusion Limit: | 4 x 106 Da |
Max. Temp. (ºC): | 140 |
Shipping Solvent: | THF |
P/N | Description | Particle size | Housing material | ID (mm) | Length (cm) |
0017362 | TSKgel GMHHR-L | 5 µm | Stainless Steel | 7.8 | 30 |
0017369 | Guard Column for P/N 0017362 | 5 µm | Stainless Steel | 6 | 4 |
TSKgel GMHHR-H(S) HT mixed bed
Matrix: | polystyrene-divinylbenzene |
Particle Size (mean): | 13 µm |
Pore size (mean): | mixed |
Exclusion Limit: | < 4 x 108 Da |
Max. Temp. (ºC): | 140 |
Shipping Solvent: | ODCB |
P/N | Description | Particle size | Housing material | ID (mm) | Length (cm) |
0018393 | TSKgel GMHHR-H(S) HT | 13 µm | Stainless Steel | 7.8 | 30 |
0018397 | Guard column for P/N 0018393 | 13 µm | Stainless Steel | 7.5 | 7.5 |
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